UPSI Digital Repository (UDRep)

Modified synthesis of edge scrolled reduced graphene oxide with high surface area

AVAILABLE Article 501 Views
Scan QR Code to share or view item link:

Digital Assets & Download Files
Login required to access this item.
General Information
Title
Modified synthesis of edge scrolled reduced graphene oxide with high surface area
Type
Article
Main Author
R. Rajesh, K. Balkis Ameen, K. Rajasekar,
Subject
Q Science (General)
ISSN
2289-7070
Language Code
eng
Bibliographic Details
Place of Production
Universiti Pendidikan Sultan Idris
Year of publication
2016

Abstract

Synthesis of graphene with the high surface area has been very attractive for various energy storage applications. In this work, we describe a scalable method for producing edge scrolled reduced graphene oxide (r-GO) with the high surface area by modified Hummer’s method. Strong acid treated graphite flakes were used to synthesis reduced graphene oxide. Few layered, edge scrolled reduced graphene oxide was obtained by low temperature (200℃) thermal treatment in a hydrogen atmosphere. The formation of few layered graphitic structure of reduced graphene oxide was confirmed by TEM analysis. The specific surface area of the reduced graphene oxide was measured by nitrogen adsorption technique. The reduced graphene oxide derived from acid treated graphite flakes exhibits high surface area (~ 500 m2/g) than non acid treated graphite flakes (214.4 m2/g).

References

1. Brownson, D. A., Kampouris, D. K., & Banks, C. E. (2011). An overview of graphene in energy production and storage applications. Journal of Power Sources, 196(11), 4873-4885. 2. Chen, G., Weng, W., Wu, D., Wu, C., Lu, J., Wang, P., & Chen, X. (2004). Preparation and characterization of graphite nanosheets from ultrasonic powdering technique. Carbon, 42(4), 753-759. 3. Das, T. K., & Prusty, S. (2013). Graphene-based polymer composites and their applications. Polymer-Plastics Technology and Engineering, 52(4), 319-331. 4. Hummers Jr, W. S., & Offeman, R. E. (1958). Preparation of graphitic oxide. Journal of the American Chemical Society, 80(6), 1339-1339. 5. Korkut, S., Roy-Mayhew, J. D., Dabbs, D. M., Milius, D. L., & Aksay, I. A. (2011). High surface area tapes produced with functionalized graphene. ACS nano, 5(6), 5214-5222. 6. Razieh, J., Jahanshahi, M., Rashidi, A., & Ghoreyshi, A. A. (2013). Synthesize and characterization of graphene nanosheets with high surface area and nano-porous structure. Applied surface science, 276, 672-681. 7. Shahriary, L., & Athawale, A. A. (2014). Graphene oxide synthesized by using modified hummers approach. IJREEE, 2(1), 58-63. 8. Sun, L. W., Zhao, J., Zhou, L. J., & Li, G. D. (2013). Facile hydrothermal preparation of graphene oxide nanoribbons from graphene oxide. Chemical Communications, 49(54), 6087-6089. 9. Wang, J., & Ellsworth, M. (2009). Graphene aerogels. ECS Transactions, 19(5), 241-247. 10. Worsley, M. A., Kucheyev, S. O., Mason, H. E., Merrill, M. D., Mayer, B. P., Lewicki, J., ... & Satcher, J. H. (2012). Mechanically robust 3D graphene macroassembly with high surface area. Chemical Communications, 48(67), 8428-8430. 11. Xu, Y., Sheng, K., Li, C., & Shi, G. (2010). Self-assembled graphene hydrogel via a one-step hydrothermal process. ACS Nano, 4(7), 4324-4330. 12. Zhang, L., Zhang, F., Yang, X., Long, G., Wu, Y., Zhang, T & Chen, Y. (2013). Porous 3D graphene-based bulk materials with exceptional high surface area and excellent conductivity for supercapacitors. Scientific reports, 3.


Installed and configured by Bahagian Automasi, Perpustakaan Tuanku Bainun, Universiti Pendidikan Sultan Idris
If you have enquiries, kindly contact us at pustakasys@upsi.edu.my or 016-3630263. Office hours only.