Simultaneously determination of bisphenol A and uric acid by zinc/aluminum-layered double hydroxide-2-(2,4dichlorophenoxy) propionate paste electrode

Illyas Md Isa

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Type :	article
Subject :	Q Science
Main Author :	Illyas Md Isa
Additional Authors :	Nurul Syahida Mat Rais Norhayati Hashim Mohamad Idris Saidin Siti Nur Akmar Mohd Yazid Mohamad Syahrizal Ahmad Rahadian Zainul Suyanta Siriboon Mukdasai
Title :	Simultaneously determination of bisphenol A and uric acid by zinc/aluminum-layered double hydroxide-2-(2,4dichlorophenoxy) propionate paste electrode

Place of Production :	Tanjong Malim
Publisher :	Fakulti Sains dan Matematik
Year of Publication :	2019
Corporate Name :	Universiti Pendidikan Sultan Idris

Full Text : Universiti Pendidikan Sultan Idris

A novel zinc/aluminium-layered double hydroxide-2-(2,4-dichlorophenoxy) propionate (Zn/Al-LDHDPPA) nanocomposite to modify with multi-walled carbon nanotube (MWCNT) paste electrode for simultaneously determination of uric acid and bisphenol A. The Zn/Al-LDH-DPPA/MWCNT morphology was carried out by a scanning electron microscope and transmission electron microscope, electrode-electrolyte interface properties were examined by electrochemical impedance spectroscopy, and electrochemical responses thoroughly investigated by square-wave voltammetry. The electrode established linear plot for uric acid and bisphenol A from 5.0 x 10—6 M to 7.0 x 10—4 M (R2 = 0.9980) and (R2 = 0.9960) and the detection limits were 7.95 x 10—7 M and 8.71 x 10—7 M (S/N=3). The asprepared sensor is reproducible, highly stable, sensitive as well as ascribed good anti-interference ability. The Zn/Al-LDH-DPPA/MWCNT electrode is applicable to evaluate simultaneously determination of UA and BPA in lake, river and, urine samples with good percentage recovery.

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