Surfactant-assisted imidacloprid intercalation of layered zinc hydroxide nitrate:synthesis, characterisation and controlled resease formulation

Norhayati Hashim

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Type :	article
Subject :	Q Science (General)
Main Author :	Norhayati Hashim
Additional Authors :	Sharifah Norain Mohd Sharif Illyas Md Isa Suriani Abu Bakar Mohamad Idris Saidin Mohamad Syahrizal Ahmad
Title :	Surfactant-assisted imidacloprid intercalation of layered zinc hydroxide nitrate:synthesis, characterisation and controlled resease formulation

Place of Production :	Tanjong Malim
Publisher :	Fakulti Sains dan Matematik
Year of Publication :	2019
Corporate Name :	Universiti Pendidikan Sultan Idris
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Abstract : Universiti Pendidikan Sultan Idris

A neutrally charged insecticide, imidacloprid (IC), has been intercalated into zinc hydroxide nitrate (ZHN) with the assistance of sodium dodecylsulphate (SDS). The presence of SDS assists the intercalation of IC by forming a hydrophobic region in the interlayer gallery of ZHN. The intercalated compound, ZHN–SDS–IC, was characterised using powder X-ray difraction (PXRD), thermogravimetric analysis, Fourier transform infrared spectroscopy, elemental analysis, feld emission scanning electron microscopy, and gas sorption analysis. The PXRD studies demonstrated intercalation peaks at lower 2θ, which confrmed the intercalation of IC and SDS in the interlayer gallery of ZHN. The release and kinetic studies of ZHN–SDS–IC reveals that the IC were successfully released in controlled manner (with release time up to 1478 min), and were governed by pseudo second order kinetic model. The ZHN–SDS–IC synthesised is hopefully benefcial in overcoming the consequences of excessive usage of insecticide in paddy cultivation.

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