UPSI Digital Repository (UDRep)
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UPSI Digital Repository (UDRep)
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| Abstract : Universiti Pendidikan Sultan Idris |
| Ultrasonic-assisted extraction (UAE) on the Cassia sieberiana root was optimised by a three-factor-three-level Box-Behnken design (BBD). A single factor experiment revealed the logic ranges for the UAE parameters for extraction time, temperature and solvent to sample ratio were 10-60 min, 30-60 C and 10-30 mL/g, respectively. The BBD showed that a second-order polynomial model produced a satisfactory fitting of the experimental data (R2 = 0.9917, P < 0.001) with regards to extraction yield. The optimal UAE conditions were 29 min, 45 C and 16.79 mL/g. Under the optimised conditions, the UAE yielded 1.28 � 0.7% of C. sieberiana root extract as to 0.69 � 1.1% obtained by maceration and 0.82 � 0.5% obtained by Soxhlet extraction. The results affirmed that the BBD was suitable in establishing the optimum UAE conditions for a maximum extraction yield while being more efficient and rapid than conventional methods (maceration and Soxhlet extraction). ? 2021 Inderscience Enterprises Ltd.. All rights reserved. |
| References |
Abdullahi, A. B., Lawan, B. B., Mohammed, K., Joshua, L., & Hauwa, M. M. (2013). Acute toxicity study on aqueous extract of the leaf of cassia sieberiana D.C. (caesalpiniaceae) in albino rats. Int.J.Nig.Soc.Exp.Bio, 25, 124-126. Retrieved from www.scopus.com Ahamad, J., Amin, S., & Mir, S. R. (2015). Optimization of ultrasound-assisted extraction of charantin from momordica charantia fruits using response surface methodology. Journal of Pharmacy and Bioallied Sciences, 7(4), 304-307. doi:10.4103/0975-7406.168032 Altemimi, A., Watson, D. G., Kinsel, M., & Lightfoot, D. A. (2015). Simultaneous extraction, optimization, and analysis of flavonoids and polyphenols from peach and pumpkin extracts using a TLC-densitometric method. Chemistry Central Journal, 9(1) doi:10.1186/s13065-015-0113-4 Cacace, J. E., & Mazza, G. (2003). Mass transfer process during extraction of phenolic compounds from milled berries. Journal of Food Engineering, 59(4), 379-389. doi:10.1016/S0260-8774(02)00497-1 Ebrahimi-Najafabadi, H., Leardi, R., & Jalali-Heravi, M. (2014). Experimental design in analytical chemistry -part I: Theory. Journal of AOAC International, 97(1), 3-11. doi:10.5740/jaoacint.SGEEbrahimi1 Esclapez, M. D., García-Pérez, J. V., Mulet, A., & Cárcel, J. A. (2011). Ultrasound-assisted extraction of natural products. Food Engineering Reviews, 3(2), 108-120. doi:10.1007/s12393-011-9036-6 Hussain, A. I., Chatha, S. A. S., Noor, S., Khan, Z. A., Arshad, M. U., Rathore, H. A., & Sattar, M. Z. A. (2012). Effect of extraction techniques and solvent systems on the extraction of antioxidant components from peanut (arachis hypogaea L.) hulls. Food Analytical Methods, 5(4), 890-896. doi:10.1007/s12161-011-9325-y Jibril, S., Sirat, H. M., & Basar, N. (2017). A new stilbene from the root of cassia sieberiana D.C. (fabaceae). Natural Product Communications, 12(7), 1095-1098. doi:10.1177/1934578x1701200723 Jibril, S., Sirat, H. M., & Basar, N. (2017). Bioassay-guided isolation of antioxidants and α-glucosidase inhibitors from the root of cassia sieberiana D.C. (fabaceae). Records of Natural Products, 11(4), 406-410. Retrieved from www.scopus.com Khala, H. M., Karumi, Y., & Buratai, L. B. (2014). Studies on the hepatotoxic effects of cassia sieberiana D.C. stem bark aqueous extract in rats. Academia J.Med.Pl, 2, 49-56. Retrieved from www.scopus.com Kpegba, K., Agbonon, A., Petrovic, A. G., Amouzou, E., Gbeassor, M., Proni, G., & Nesnas, N. (2011). Epiafzelechin from the root bark of cassia sieberiana: Detection by DART mass spectrometry, spectroscopic characterization, and antioxidant properties. Journal of Natural Products, 74(3), 455-459. doi:10.1021/np100090e Kuo, C. -., Chen, B. -., Liu, Y. -., Chang, C. -. -., Deng, T. -., Chen, J. -., & Shieh, C. -. (2014). Optimized ultrasound-assisted extraction of phenolic compounds from polygonum cuspidatum. Molecules, 19(1), 67-77. doi:10.3390/molecules19010067 Li, W., Wang, Z., Sun, Y. -., Chen, L., Han, L. -., & Zheng, Y. -. (2011). Application of response surface methodology to optimise ultrasonic-assisted extraction of four chromones in radix saposhnikoviae. Phytochemical Analysis, 22(4), 313-321. doi:10.1002/pca.1282 Liu, J. -., Li, L. -., & He, G. -. (2016). Optimization of microwave-assisted extraction conditions for five major bioactive compounds from flos sophorae immaturus (cultivars of sophora japonica L.) using response surface methodology. Molecules, 21(3) doi:10.3390/molecules21030296 Majeed, M., Hussain, A. I., Chatha, S. A. S., Khosa, M. K. K., Kamal, G. M., Kamal, M. A., . . . Liu, M. (2016). Optimization protocol for the extraction of antioxidant components from origanum vulgare leaves using response surface methodology. Saudi Journal of Biological Sciences, 23(3), 389-396. doi:10.1016/j.sjbs.2015.04.010 Manan, F. M. A., Rahman, I. N. A., Marzuki, N. H. C., Mahat, N. A., Huyop, F., & Wahab, R. A. (2016). Statistical modelling of eugenol benzoate synthesis using rhizomucor miehei lipase reinforced nanobioconjugates. Process Biochemistry, 51(2), 249-262. doi:10.1016/j.procbio.2015.12.002 Mavituna, F. (1992). Applications of plant biotechnology in industry and agriculture. Recent Advances in Biotechnology, , 209-226. Retrieved from www.scopus.com Mohamad, N., Huyop, F., Aboul-Enein, H. Y., Mahat, N. A., & Waha, R. A. (2015). Response surface methodological approach for optimizing production of geranyl propionate catalysed by carbon nanotubes nanobioconjugates. Biotechnology and Biotechnological Equipment, 29(4), 732-739. doi:10.1080/13102818.2015.1034177 Nartey, E. T., Ofosuhene, M., & Agbale, C. M. (2012). Anti-ulcerogenic activity of the root bark extract of the african laburnum "cassia sieberiana" and its effect on the anti-oxidant defence system in rats. BMC Complementary and Alternative Medicine, 12 doi:10.1186/1472-6882-12-247 Prado, J. M., Veggi, P. C., Angela, M., & Meireles, A. (2017). Scale-up issues and cost of manufacturing bioactive compounds by supercritical fluid extraction and ultrasound assisted extraction. Global food security and wellness (pp. 377-433) doi:10.1007/978-1-4939-6496-3_20 Retrieved from www.scopus.com Sarker, S. D., Latif, Z., & Gray, A. I. (2006). Natural Products Isolation, Retrieved from www.scopus.com Spigno, G., Tramelli, L., & De Faveri, D. M. (2007). Effects of extraction time, temperature and solvent on concentration and antioxidant activity of grape marc phenolics. Journal of Food Engineering, 81(1), 200-208. doi:10.1016/j.jfoodeng.2006.10.021 Toma, I., Karumi, Y., & Geidam, M. A. (2009). Phytochemical screening and toxicity studies of the aqueous extract of the pods pulp of cassia sieberiana DC. (cassia kotchiyana oliv.). Afr J Pure Appl Chem, 3(2), 026-030. Retrieved from www.scopus.com Wang, L., & Weller, C. L. (2006). Recent advances in extraction of nutraceuticals from plants. Trends in Food Science and Technology, 17(6), 300-312. doi:10.1016/j.tifs.2005.12.004 Zou, Y., Jiang, A., & Tian, M. (2015). Extraction optimization of antioxidant polysaccharides from auricularia auricula fruiting bodies. Food Science and Technology (Brazil), 35(3), 428-433. doi:10.1590/1678-457X.6712 |
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