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UPSI Digital Repository (UDRep)
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| Total records found : 1 |
| Simplified search suggestions : Iman Nur Fathihah Abdul Aziz |
| 1 | 2019 Thesis | Synthesis and characterization of zinc layered hydroxide intercalated with 4-aminobenzoic acid as sunscreen formulation Iman Nur Fathihah Abdul Aziz The aims of this study were to synthesis and characterize zinc layered hydroxide
intercalated with 4-aminobenzoic acid (ZAB) as a sunscreen formulation. ZAB was successfully
synthesized from 4-aminobenzoic acid (4-AB) and zinc oxide (ZnO) precursor using direct
method. The intercalation of compound was confirmed by using powder x-ray diffraction (PXRD)
pattern with a basal spacing of 23.2 Å at lower 2θ angle. The result was supported by fourier
transform infrared (FTIR) spectrum where the signal of carboxyl and amine functional groups were
observed at 1518 and 1174 cm?¹, respectively. Thermogravimetric analysis and deferential
thermal gravimetric (TGA/DTG) showed that ZAB material was more stable compared to pure
4-AB. Carbon composition in the material acquired from carbon, hydrogen, nitrogen and
sulphur (CHNS) analysis was 19.2%. This composition is close to t..... 2635 hits |